SY/T 0413

SY/T 0413-2002: Technical Standard for Polyethylene Coating of Buried Steel Pipelines

1. Standard Definition and Background

SY/T 0413-2002:Released by National Economic and Trade Commission of China on May 28, 20021 implemented on August 1, 2002. I This petroleum industry standard (PS) is developed by Petroleum Engineering Construction Standardization Committee and formulated by CNPC Engineering Technology R&D Institute. It has replaced SY/T 4013-1995 and reached consensus standard for corrosion protection of buried steel pipe epoxy powder coating of polyethylene recommend standard.

Key Objectives: Long-term corrosion protection Structure support in soil environments through:

Standardisation of 2 (2PE) and 3 (3PE) interceptor coating systems

Performance levels of workable material

Quality control protocols

Field application procedures

Historical Context:

Developed during China’s Pipeline construction (1990s–early 2000s)

Adopted German DIN 3067-1991 with variation for Chinese climatic conditions

Replaced by GB/T 23257 (2010) and still in use for legacy projects

2. Scope of Application

2.1 Service Environments

Coating TypeTemp. RangePrimary Applications
Normal (N-Type)-30°C to 50°COil/Gas/Water transmission (non-aggressive soils)
High-Temp (H-Type)-30°C to 70°CGeothermal/desert pipelines

2.2 Pipeline Systems Covered

Energy Transport: Crude oil, natural gas, refined products (design pressure ≤4.0 MPa)

Municipal Utilities: Water supply/drainage, irrigation networks

Industrial Lines: Slurry transport, steam pipelines

3. Coating Structure & Material Requirements

3.1 Coating Systems

StructureLayersKey Features
2PE① Adhesive + ② PECost-effective; moderate corrosion resistance
3PE① FBE + ② Adhesive + ③ PESuperior adhesion/mechanical protection

3.2 Thickness Requirements

Table: Minimum Coating Thickness (mm)

Pipe DN (mm)FBE (μm)Adhesive (μm)PE Layer
Std (G)Reinf (S)
<100170–2501.82.5
100–80060–150170–2503.03.7

3.3 Material Specifications

Epoxy Powder (FBE):

Gel time (200°C): ≤30 sec

Cathodic disbondment (65°C/48h): ≤10 mm

Adhesion: ≤Grade 2 (cross-cut test)

Adhesive:

Peel strength: ≥35 N/cm (2PE), ≥60 N/cm (3PE) at 20°C

Softening point: ≥90°C (2PE), ≥80°C (3PE)

Polyethylene:

Density: ≥0.940 g/cm³

Carbon black: 2.0–2.4%

Thermal aging (100°C): ΔMFR ≤35% after 2,400h (N-Type) or 4,800h (H-Type)

4. Manufacturing & Construction

4.1 Surface Preparation

Abrasive cleaning: Sa 2.5 (near-white metal)

Anchor profile: 50–75 μm

Preheating: 40–60°C (max 4h before coating)

4.2 Coating Application

ProcessParameters
FBE SprayingVoltage: 40–80 kV; Thickness: 60–150 μm
Adhesive/PE ExtrusionTemp: 150–170°C; Weld overlap: ≥10 mm
CoolingWater-cooled to ≤60°C

End Treatment:

100–150 mm uncoated zone at pipe ends

Bevel angle: ≤30°

Temporary rust inhibitor: ≥50 μm DFT

5. Testing & Inspection

5.1 Performance Requirements

TestRequirement
Impact ResistanceNo cracking at 24 J
Cathodic Disbondment≤15 mm (2PE), ≤10 mm (3PE) at 65°C/48h
Bend TestNo cracking at 2.5° bend
Peel Strength≥35 N/cm (2PE), ≥60 N/cm (3PE) at 20°C

5.2 Quality Control

100% inspection: Visual + holiday detection (25 kV)

Thickness checks: 1st/5th/10th pipe per batch, then 1 per 10 pipes

Sampling frequency:

Peel test: 1 per 50 pipes

Mechanical properties: Per 8h shift

6. Engineering Applications & Limitations

6.1 Major Projects

West-East Gas Pipeline I: 3,000+ km with 3PE coating (15+ years service)

Sino-Russian Crude Pipeline: H-Type coating for -45°C environments

Urban Gas Networks: 2PE coatings for DN≤300 pipes (40% cost reduction)

6.2 Technical Limitations

Thickness control: Incompatible with overlap zones in spiral application

Testing duration: 2,400h thermal aging test impractical for QC

Environmental gaps: No VOC/heavy metal restrictions

Adhesive metrics: Missing tensile strength/elongation criteria

7. Technical Legacy & Evolution

SY/T 0413-2002 laid the foundation for China’s modern pipeline coating systems by:

Establishing material/process benchmarks for 2PE/3PE coatings

Reducing corrosion failures by ~70% during 2002–2010

Enabling localization of PE/epoxy materials (50% cost reduction by 2005)

Advancements:

Smart coatings: Embedded sensors for real-time monitoring

Self-healing systems: Microcapsule-based damage repair

Eco-formulations: VOC-free adhesives, recycled PE

Guidance:

For in-service pipelines coated per SY/T 0413:

Monitor thermal aging (MFR change ≤35%)

Verify cathodic protection compatibility

Replace field joints after 15 years

New projects should adopt GB/T 23257-2017.

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